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Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals

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DOI

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Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals. / Armstrong, Jennifer A.; Friis, Henrik; Lieb, Alexandra; Finch, Adrian A.; Weller, Mark T.

In: American Mineralogist, Vol. 95, No. 4, 04.2010, p. 519-526.

Research output: Contribution to journalArticle

Harvard

Armstrong, JA, Friis, H, Lieb, A, Finch, AA & Weller, MT 2010, 'Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals' American Mineralogist, vol. 95, no. 4, pp. 519-526. https://doi.org/10.2138/am.2010.3276

APA

Armstrong, J. A., Friis, H., Lieb, A., Finch, A. A., & Weller, M. T. (2010). Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals. American Mineralogist, 95(4), 519-526. https://doi.org/10.2138/am.2010.3276

Vancouver

Armstrong JA, Friis H, Lieb A, Finch AA, Weller MT. Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals. American Mineralogist. 2010 Apr;95(4):519-526. https://doi.org/10.2138/am.2010.3276

Author

Armstrong, Jennifer A. ; Friis, Henrik ; Lieb, Alexandra ; Finch, Adrian A. ; Weller, Mark T. / Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals. In: American Mineralogist. 2010 ; Vol. 95, No. 4. pp. 519-526.

Bibtex - Download

@article{db47870630f1424e9d1ba914fbeca214,
title = "Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals",
abstract = "Structural analysis, using neutron powder diffraction (NPD) data on small quantities (<300 mg) and in combination with single-crystal X-ray diffraction (SXD) data, has been employed to determine accurately the position of hydrogen and other light atoms in three rare beryllate minerals, namely bavenite, leifite/IMA 2007-017, and nabesite. For bavenite, leifite/1MA 2007-017, and nabesite, significant differences in the distribution of H, as compared to the literature using SXD analysis alone, have been found. The benefits of NPD data, even with small quantities of H-containing materials, and, more generally, in applying a combined SXD-NPD method to structure analysis of minerals are discussed, with reference to the quality of the crystallographic information obtained.",
author = "Armstrong, {Jennifer A.} and Henrik Friis and Alexandra Lieb and Finch, {Adrian A.} and Weller, {Mark T.}",
year = "2010",
month = "4",
doi = "10.2138/am.2010.3276",
language = "English",
volume = "95",
pages = "519--526",
journal = "American Mineralogist",
issn = "0003-004X",
publisher = "Mineralogical Society of America",
number = "4",

}

RIS (suitable for import to EndNote) - Download

TY - JOUR

T1 - Combined single-crystal X-ray and neutron powder diffraction structure analysis exemplified through full structure determinations of framework and layer beryllate minerals

AU - Armstrong, Jennifer A.

AU - Friis, Henrik

AU - Lieb, Alexandra

AU - Finch, Adrian A.

AU - Weller, Mark T.

PY - 2010/4

Y1 - 2010/4

N2 - Structural analysis, using neutron powder diffraction (NPD) data on small quantities (<300 mg) and in combination with single-crystal X-ray diffraction (SXD) data, has been employed to determine accurately the position of hydrogen and other light atoms in three rare beryllate minerals, namely bavenite, leifite/IMA 2007-017, and nabesite. For bavenite, leifite/1MA 2007-017, and nabesite, significant differences in the distribution of H, as compared to the literature using SXD analysis alone, have been found. The benefits of NPD data, even with small quantities of H-containing materials, and, more generally, in applying a combined SXD-NPD method to structure analysis of minerals are discussed, with reference to the quality of the crystallographic information obtained.

AB - Structural analysis, using neutron powder diffraction (NPD) data on small quantities (<300 mg) and in combination with single-crystal X-ray diffraction (SXD) data, has been employed to determine accurately the position of hydrogen and other light atoms in three rare beryllate minerals, namely bavenite, leifite/IMA 2007-017, and nabesite. For bavenite, leifite/1MA 2007-017, and nabesite, significant differences in the distribution of H, as compared to the literature using SXD analysis alone, have been found. The benefits of NPD data, even with small quantities of H-containing materials, and, more generally, in applying a combined SXD-NPD method to structure analysis of minerals are discussed, with reference to the quality of the crystallographic information obtained.

U2 - 10.2138/am.2010.3276

DO - 10.2138/am.2010.3276

M3 - Article

VL - 95

SP - 519

EP - 526

JO - American Mineralogist

T2 - American Mineralogist

JF - American Mineralogist

SN - 0003-004X

IS - 4

ER -

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ID: 38882842